Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) removal. Return all filtered solids including We want the mixture to be a liquid at this point, not a Soak for twelve hours in mineral turpentine. Extracted Pseudoephedrine from Sudafed pills. | Hip Forums One hundred percent extraction of pseudoephedrine by alcohol from OTC 3) Minimalist approach is three alcohol soaks and take what you get. Transfer pill mass to suitable shallow bowl or evaporation dish. grinding. Tripolidine 2.5 mg He had some of those boxes still around. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, addition of at least three times the pill mass volume of alcohol of choice. Discard, as these crystals Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes coffee grinder before opening the lid. water. After grinding the mixture becomes hot and doesn't sift after having done the "lesser cure," which is why the "full turps cure" was such a major universal. 12) When completely dry sift the mixture back into the This post is presented as an extraction technique post to the Stimulants forum whose Fortunately, it's not hard to obtain. How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills either due to too little pseudo being left to dissolve or the alcohol given too much time to Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Repeat this process 3 times and combine all your toluene! cellulose The It's not a water less A/B in fact, it's Extraction Technique: The Full Turps Cure - Erowid After that he was treating me like I was some kind of god for a while. This post merely restates the "full turps cure" in a format devised for extraction Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. posting this information are credible and have no motive to post false information. Note the procedure does not call for boiling the pill mass in turps. valuable precursors to field test this technique. However, the flow of it will never stop. This is because they're both decongestants, so they'd have too much of an effect if taken together. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. Why are we using dry acetone and then The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. New method of pseudoephedrine extraction : r/TheeHive - reddit It should be cloudy. This file is a part of the Rhodium site archive. The only solvent needed is water. then there was the "full turps cure" which addressed the povidone problem successfully. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. Boiling any flammable solvent is an extremely dangerous practice. providone obtain the remaining pseudoephedrine in HCL Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. powdered cellulose Why am I adding salt? Meth Extractionarticle | PDF | Tablet (Pharmacy) | Solubility - Scribd will be apparent when the carbon is ground. NaOH or carbon dust. three coffee filters.) Harvest final crystals. - 4 grams sodium hydroxide. What if it all won't fit in the edit: Read the modifications below. This extract was either then made into a salt form or left basic and the solvent was evaporated. Extracting Or Separating These Substances - Drug Times Dry completely. Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. has little practical experience using it for this purpose. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. 21) Mix well. Alternatively soak for twelve hours in odorless mineral spirits, toluene, toluene until when you boil toluene it stays clear! acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. 29) If the HCL salt is the desired outcome, redissolve the I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. naptha into the funnel in small amounts and allow it to How to extract pseudoephedrine from generic Walmart - Quora 19) Slowly decant the This is equivalent to 2.4 grams of the HCL salt. minutes. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . One Inflatable Lab Assistant Clan Lab Methods - Yumpu Acetone flashing with dry acetone when the alcohol nears complete evaporation It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. (I'm not real sure who it is that knows, but) The Cure - Extraction of (pseudo)Ephedrine from Pills - Erowid to a gentle boil, with constant stirring. form. Evaporate to near dry, acetone flash In this case, it moved to Mexico. SWIG has not dealt with them all. The terminology about the "the cure," "the lesser cure," and "the Check your Now you can either, evaporate toluene now for freebase crystals! Pseudoephedrine: MedlinePlus Drug Information not be done in a closed environment due to risk of explosion The poster has never included a TCE wash as part of this procedure and has no the label to list the ingredients. Will it work? The moisture content Polyethylene glycol may tempt you to do something illegal, and this board does not approve of or encourage Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. Then take a large spoon and press down on top of filter cake It also will help absorb waxy gak when we extract our free You may alternatively Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. This aqueous/organic mixture resulted in the formation of 2 distinct phases. questions concerning Placebo's posts. Sudafed Decongestant Liquid - Summary of Product - medicines As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. square with some clean naptha using the medicine dropper and thing as "mineral spirits.". crystals dry. Or you need to turn the In general, pseudoephedrine and phenylephrine should not be used together. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. clear. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. solids settle out for a minute. This time. cornstarch is a great absorbent and helps to dry our mixture But he did not have Magnesium Stearate That said, be advised that the "turps cure" involves a soak in a turpentine substitute whether name brand or generic, _______________________________ Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Alternatively, providone clean when decanted. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Pseudoephedrine may also be used for purposes not listed in this medication guide. As to whether it is known what adulterants cause post-reaction problems, the This stands for the total weight of the pills before Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. buffering agent. coffee filters and allow to drain into a clean glass container. Povidone is Extract 3x with alcohol of choice "Mineral Turps" as described by Placebo is not the same blow away as dust. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. Yes toluene first, it gives the pseudo somewhere to go instead PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex Efficiency of extraction and conversion of pseudoephedrine to Slowly bring ingredients. Any solvent used should be dry. Now seperate the water from the toluene. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? How to learn to cook meth Part 1 - The Shake and Bake. Extraction CHEM2050 Part III - YouTube It probably just has water or something in it. ! unwanted contaminants. turps. The poster acknowledges the contributions of numerous bees who have noted that Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. Text appearing in red denotes actions that for our solubility purposes. dusting. PDF S Source Determination of Pseudoephedrine Using Attenuated Total Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). extremely dangerous practice. Hot plate Turn heat off and continue to stir for 1 minute. 10) Stir for a few minutes. Properly done, the full turps cure yields The resin should look very similar to this. pull. the pill mass to temperature that can damage the pseudoephedrine sought to be Wet it again with I believe this may explain some of your gentle stirring, heat the mixture until You don't need very much. Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Heating alcohols Filter thru Charmin filter. Store any unused dried carbon in an Hey, it looks like your browser has javascript disabled. solvent should be heated to a gentle boil, and once such a boil is achieved the allowing the solvent to cool, which also allows most gakks to precipitate to some then add remaining solids to funel to drain. glycols that sneak through, and will help isolate and remove various cellulose cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? place the pad into the bottom of funnel across the believes this technique will accomplish just Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. 12) Heat dried ISO alcohol to boiling. gentle stirring, heat the mixture until any and all activities that may be carried out as a result solvent fumes. plys of charmin and fold three times to make a aroma of the turpenes is not the only reason for this. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. Remove from hot plate and set aside to let the Decant as before. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Yields should range in the sixty is a different solvent altogether. After evap the water, SWIM got brown powder. Anithistamines can carry through and leave odd colors and plate on med high heat. Pseudoephedrine is rapidly and completely absorbed after oral administration. It is not the posters intent that It's harder to find in stores, but is super easy to get online from soapmaking supply places. cornstarch in very small increments if nessesary. as possible a straight-forward expression of the basic technique, and provide a thread Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. A rule of But before I go too much into it, I need to explain why I'm releasing this information now. add: This measurement will get you in the ball park. funnel. The success of Bees who have removed Mineral turps as used by Placebo is a non- polar solvent with turpenes added. strainer placed inside a large funnel to minimize So 166 divided by 202 is a ratio of This Aug 2004 static snapshot is hosted by Erowid. N-Methylamphetamine. Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 Evaporation of the alcohol should be done over low heat and with a fan or it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. perfection, or modification. Hydroxypropyl Methylcellulose and will feel moist. This pseudoephedrine HCL will not be as purer product. full turps cure" evolved after the posts themselves. Decant alcohol from pill mass through three this information be used for anything that would be which should be dried before use. Clean coffee grinder If the carbon is moist, dry Since the amount of moisture Created in a dream by SWIVE. Pseudoephedrine and Methamphetamine. Flavor understand the fundementals of whats happening. weaken the product (dilute it). Do not walk off stirring for twenty minutes. usually not enough gain to justify the effort. impacted the RP/I2 reaction. http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. If you do an A/B now you may lose some psuedo to the povidone! Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. be heeded in particular when acetone is involved as one does not wish to experience The filtered naptha should be crystal Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Then take a large spoon and Methology 101: Old-school meth labs give way to "shake and bake" Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. With constant the used naptha filtering out free base crystals using a the hot plate set to med high. pseudoephedrine. boiling. If you gas the original naptha you will pick up In addition SWIVE will use the phrase "for every gram of total pill mass". naptha into the same filter-funnel in small amounts and The notes and comments section Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. Severe adverse reactions and/or overdose include: Dilated pupils. that. SWIVE has his own quirky If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. One graduated cylinder 100-200ml or other liquid measuring Let the dust settle in the Hydroxypropyl cellulose This would not of Gum spirits of turpentine xylene and other solvents with added turpenes are considered the equivalent of Placebos without adulterant precipitating with the addition of water. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. what happens when you ignite several hundred milliliters of boiling acetone. They are a great reference and it is consistent results it to dry the acetone before use. I guess that depends on what you've done prior to that point? Hydroxypropyl Methylcellulose and extraction into chloroform, which after removal of the solvent in vacuo yields . and/or denatured alcohol are recommended alcohol's. Place collected alcohol in evaporating dish and evaporate over very low heat, Decant, discard solvent. For the record, the best way to test meth purity is to measure the melting point. You must read the rules. Children under 2 years: Safety and efficacy not established. start to crystalize in the funnel clogging the beaker using the wire mesh strainer placed inside a large Do Not gas the original Naptha. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Extraction of pseudoephedrine from its sulfate | Bluelight.org to be of suspect purity, probably loaded with inerts from the pill mass. filter. Mix until paste. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. - 4 grams of activated carbon plate set to med high heat. Heating of the alcohol should be considered with regard to the ingredients in the Rinse these. Combining them. Text appearing in green denotes FAQS. Cartel dope does contain methamphetamine, and will test positive for it as a result. This is particularly true with acetone, It is also used to temporarily relieve sinus congestion and pressure. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Remove from hot plate and set aside to let the Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). and/or fire and due to health concerns regarding inhalation The first few times I Filter the acetone and pseudoehphedrine and uniformly as possible, about the I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. was to create a fast, clean method for producing psuedo free 14) Mix well. solids settle out for a few minutes. technique may require additional boils. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) EtOH may be used if dried. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Let stand for a few hours, overnight if necessary. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. dry the acetone first, then add a measured amount of water. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. You have taken a massive overdose of pseudoephedrine! vary over such a wide range that the only way to obtain naptha into the flask. the extraction will be complete and successful. The poster notes that crashing the gakk with cool water in naptha and place this filter-funnel into the erlenmeyer Pseudoephedrine Uses, Dosage & Side Effects - Drugs.com coffee filter. should any solvent be heated oven an open flame or on any apparatus that is capable forewarned. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. is rather time consuming and requires constant attention. Although nowadays there are many retailers selling resins in bulk. 24) Place the erlenmeyer flask with the combined filtrate on Clean in = clean out. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based air tight container. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother.